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再造烟叶的纤维和组织微观结构及热解性能分析

Analysis of fiber, microstructure and pyrolysis performance of reconstituted tobacco

  • 摘要: 为了研究造纸法再造烟叶内部的纤维结构和组织疏松特性及其对燃烧性能的影响,通过纤维分析仪分析了再造烟叶的纤维形态和分布,采用扫描电镜(SEM)对再造烟叶的纤维、烟梗导管和浆料堆积层状组织的微观结构进行了分析和比较,探索了不同产品纤维和组织结构差异所引起的物理性能和热解性能的差异。结果表明:①不同产品的纤维平均长度、宽度以及长度分布上有较大差别,几种样品纤维的平均长度为0.95~1.44 mm,平均宽度为21.0~49.6 μm。②在微观结构上观察到2种形貌截然不同的纤维:一种为柔软和卷曲的扁状空心纤维,交织能力好,另一种为硬挺和交织能力差的圆形实心纤维。③未解离烟梗导管壁的厚度和堆积层状组织的微观孔隙率在不同产品之间也存在较大差异。再造烟叶的长纤维比例高有利于提高产品的抗张强度,纤维宽度大则使松厚度值增加。微观结构疏松性良好的产品,表现出较低的抗张强度和很高的透气度。微观结构疏松多孔、纤维木质化程度低的再造烟叶,具有较低的热分解温度和较高的热失重速率。纤维的构成和微观结构的疏松性对再造烟叶的热解性能有重要影响。

     

    Abstract: In order to investigate the fiber structure, textural porosity and their influences on combustion property of paper-making process reconstituted tobacco, the morphology and distribution of fiber in reconstituted tobacco were analyzed by a fiber tester, and the microstructure of fibers, tobacco stem vessels and pulp stacking stratifications were observed and compared with scanning electron microscope (SEM). The differences in physical property and pyrolysis behavior between different reconstituted tobacco products caused by fibers and textural structures were researched. The results showed that: 1) The average length, width and length distribution of fibers in different samples differed greatly, the average length of fibers in the samples ranged from 0.95 to 1.44 mm, the average width from 21.0 to 49.6 μm. 2)Two microstructurally different fibers were observed, the one was soft and crimped with flat and hollow microstructure and possessed better interweaving property, the other was stiff with round and solid microstructure. 3) There were obvious differences in the vessel wall thickness of undissociated tobacco stem and the microporosity of stratifications between difference samples. High proportion of long fiber increased tensile strength, wider fiber increased bulk thickness. The samples with open microstructure presented lower tensile strength and higher air permeability; and the samples with open and porous microstructure and low fiber lignification degree had lower pyrolysis temperature and higher weight loss rate. The fiber composition and microporosity affect the pyrolysis behavior of reconstituted tobacco significantly.

     

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