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制丝线烟丝质量在线监测近红外模型的建立与应用

Establishment and application of NIR models for online cut tobacco quality monitoring in primary processing

  • 摘要: 为实现烟丝质量的在线监测,采用近红外光谱技术和化学计量学模型转移方法开发了一种快速获得在线近红外定量模型的方法。采用转速可控的转盘模拟烟丝传送带运行,以此获得模型转移所需的标准样品,运用化学计量学光谱空间转换法(SST)将烟叶粉末化学组分的离线预测模型传递为烟丝化学组分的在线预测模型,并利用转移后的在线预测模型实现了烟丝烟碱和总糖的在线监测。结果表明,光谱空间转换法能够较好地消除离线光谱和在线光谱之间的系统性差异,在线模型和离线模型对同一样品的平均预测误差在5%以内,而实现该模型转移所需的实际工作量可在一天内完成。

     

    Abstract: In order to realize online cut tobacco quality monitoring, a method for fast establishing online NIR quantitative models was developed by NIR spectrum technique and chemometric model transformation. A speed adjustable rotating disc was used to simulate the running of a tobacco conveyor, from which the standard samples and their spectra at different conditions needed for model transformation were taken. Spectral Space Transformation (SST) was used to transform the offline prediction models for the chemical components in tobacco powder into the online prediction models for the chemical components in cut tobacco. An online experiment monitoring nicotine and total sugar in cut tobacco was conducted, the results showed that SST could effectively eliminate the systematic variation between the offline and online spectra of a sample with the average prediction error below 5%, and the model transformation could be completed within one day.

     

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