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试纸法快速检测烟叶中的镉

Rapid detection of cadmium in tobacco leaves by test paper strip

  • 摘要: 为实现烟叶样品中镉(Cd2+)的快速、实时、现场检测和筛查,以普通过滤试纸为载体,将具有特效显色反应的镉试剂通过浸渍负载到试纸上,建立了快速检测烟叶中镉质量分数的方法。通过显色观察确定适合的显色试剂,制备镉试纸,镉试纸再与不同浓度的标准镉溶液反应形成标准色阶。结果表明:①镉标准溶液浓度在0~10.0 μg/mL范围内时,试纸显色随镉离子浓度的增加颜色逐渐加深;②方法的最低检出浓度为0.5 μg/mL;③该方法具有操作简单、成本低廉、检测快速等特点,可用于烟草中镉质量分数的快速初步筛选。

     

    Abstract: In order to achieve rapid, real-time and on-site detection and screening of cadmium (Cd2+) in tobacco samples, a fast method was developed using test paper strips. The test paper was prepared by taking ordinary filter paper as a carrier, and cadmium reagents with special chromogenic reactions were absorbed by the filter paper via immersing. Appropriate chromogenic reagents for preparing the cadmium test paper were selected through observing the color changes of the test paper, and the standard color scale was determined by reacting the prepared cadmium test paper with standard cadmium solutions at different concentrations. The results showed that:1) When the concentration of cadmium standard solution was in the range of 0-10.0 μg/mL, the color of the cadmium test paper was deepened progressively with the increase of cadmium ion concentration. 2) The minimum detection concentration of cadmium ion was 0.5 μg/mL. 3) With the advantages of simple operation, low cost and rapid detection, this method was suitable for the rapid screening of cadmium content in tobacco leaf.

     

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