本平台为互联网非涉密平台,严禁处理、传输国家秘密或工作秘密

基于热分析图谱的卷烟纸质量稳定性评价与分析

Evaluation of quality consistency of cigarette paper based on thermal spectroscopic features

  • 摘要: 为分析评价卷烟纸的质量稳定性,跟踪了3家卷烟纸厂批内和批间的卷烟纸样品热分析图谱,结合标准均方根误差NRMSE量化评价卷烟纸热解燃烧差异度,并探索造成卷烟纸质量波动的原因。结果表明:①卷烟纸热分析图谱的重复性实验显示热解峰、氧化峰和碳酸钙分解峰的差异度均小于4%,说明此法可满足数据分析的要求;②卷烟纸质量波动有3种表现形式:热解峰差异度>10%,氧化峰差异度>20%,碳酸钙分解峰差异度>15%;③对比分析卷烟纸常规指标对卷烟纸热分析图谱表现形式的影响,得到对卷烟纸质量波动的影响程度排序为助剂含量>钾钠比>灰分含量;④本研究中所分析的卷烟纸样品的常规指标均在设计范围内,而不同浆料配比对热分析图谱影响表现形式与卷烟纸质量波动的表现形式一致,由此可知造成卷烟纸样品质量波动的主要原因是生产过程中阔叶木和针叶木混合不均匀性。

     

    Abstract: In order to analyze the quality consistency of cigarette paper, thermal analyses were performed on paper samples within and among batches from three cigarette paper factories. The thermal spectroscopic features were analyzed by NRMSE (normalized root mean squared error) to quantitatively evaluate the pyrolysis and combustion differences of the cigarette papers. The factors that could cause the fluctuations in paper quality were investigated. The results showed that:1) The repeatability of the thermal analysis suggested that the differences in the pyrolysis peak, oxidation peak and calcium carbonate decomposition peak were all less than 4%, which indicated that this method met the requirement for data quality analysis. 2) There were three forms of cigarette paper quality fluctuations:a pyrolysis peak difference >10%, an oxidation peak difference >20%, and a calcium carbonate decomposition peak difference >15%. 3) Through analyzing the influences of conventional paper quality indexes in relation to the patterns of thermal spectra, the paper quality indexes in the order of influence degree on the quality fluctuation were:burn additive content > potassium/sodium ratio > ash content. 4) The conventional paper quality indexes in this study were all within the designed ranges, while the influencing patterns of the different pulp ratios on the thermal analysis spectra were consistent with the quality fluctuation patterns of cigarette paper, therefore the main reason for the fluctuation of paper quality in this study was attributed to uneven mixing of hardwood and softwood fiber during production.

     

/

返回文章
返回