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3种市售枫槭浸膏关键致香成分感官导向分析

Sensory analysis of key aroma components in three commercially available maple concretes

  • 摘要: 为了阐明不同枫槭浸膏的关键致香成分及差异,以感官为导向,采用凝胶色谱分离获得了烤甜香特征组分,并以GC/MS法分析了其致香成分组成;通过测定3种市售枫槭浸膏中10种致香成分的质量分数及其在乙醇中的嗅觉阈值,获得了其香气活性值(OAV)并进行比对分析。结果表明:①枫槭浸膏烤甜香特征组分主要含有10种致香成分,分别为2,6-二甲基吡嗪、糠醛、甲基环戊烯醇酮、苯甲醇、苯乙醇、2-乙酰基吡咯、麦芽酚、2-甲酰基吡咯、葫芦巴内酯和香兰素。②3种市售枫槭浸膏中,10种致香成分总质量分数以及各种致香成分的分布情况为枫槭浸膏A与B总体上类似,二者与枫槭浸膏C差别明显。③10种致香成分在乙醇中的嗅觉阈值介于0.002~2 117.11 μg/g之间,葫芦巴内酯嗅觉阈值最低,2-甲酰基吡咯嗅觉阈值最高。3种市售枫槭浸膏中葫芦巴内酯和香兰素的OAV均远大于其他8种成分,根据OAV值大小,确定该两种成分为3种市售枫槭浸膏烤甜香的关键致香成分。

     

    Abstract: In order to investigate the key aroma components and their differences in different maple concretes, characteristic sensory components with roasted sweet aroma were separated by gel chromatography and analyzed by GC/MS. The odor activity values (OAVs) of ten aroma components in three commercially available maple concretes were calculated and compared after determining the contents of ten components and their olfactory thresholds in ethanol. The results showed that:1) The characteristic components with roasted sweet aroma in the maple concretes mainly contained ten aroma components, including 2, 6-dimethylpyrazine, furfural, methylcyclopentenolone, benzyl alcohol, phenethyl alcohol, 2-acetylpyrrole, maltol, 2-formylpyrrole, 4, 5-dimethyl-3-hydroxy-2, 5-dihydrofuran-2-one and vanillin. 2) The total contents and distributions of the 10 aroma components in maple concretes A and B were similar, while those in maple concrete C were different. 3)The olfactory thresholds of the ten aroma components in ethanol ranged from 0.002 to 2 117.11 μg/g; 2-formylpyrrole had the lowest one and 4, 5-dimethyl-3-hydroxy-2, 5-dihydrofuran-2-one had the highest. In the three maple concretes, the OAVs of 4, 5-dimethyl-3-hydroxy-2, 5-dihydrofuran-2-one and vanillin were much higher than those of the other eight components. According to the OAVs, the above two components were the key aroma components in the three maple concretes.

     

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