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近红外光谱技术在烟用香精招标质量评价中的应用

Using near-infrared spectroscopy to evaluate tobacco flavor quality during bidding

  • 摘要: 为提高烟用香精招标过程质量评价的时效,通过扫描香精的近红外光谱,采用一致性评价方法建立了395种烟用香精的质量判别模型,并应用于投标香精的质量一致性评价。结果表明:①选择波长范围为4 000~9 000 cm-1,一阶导数结合标准正态变换预处理光谱,一致性指数(CI)阈值为3;②近红外光谱相似性匹配度(M)阈值设置为90%,“拒真”的概率极低;③应用于烟用香精招标评价,92.2%的投标样品(364种)实现了快速准确的判别。模型能准确地表征样品与标样的相似性,与色谱指纹图谱分析结果一致。该方法快速准确、实用性强,适宜作为香精香料招标质量评价的快检手段。

     

    Abstract: In order to improve the efficiency of quality evaluation during the bidding process of tobacco flavors, quality discrimination models for 395 tobacco flavors were established by scanning flavors with their near-infrared spectra and backed by a consistency evaluation method. The models were applied to evaluate the quality consistency of the bidding flavors. The results showed that: 1)The selected wavelength range was from 4 000 cm-1 to 9 000 cm-1, and the first derivative was combined with the Standard Normal Variate(SNV)to pretreat the spectra with a CI(Conformity Index)threshold of 3. 2)The threshold of near-infrared spectral similarity matching degree(M)was set at 90%, so that the probability of misidentification was extremely low. 3)Using the models to evaluate the quality of the bidding flavors, 92.2% of the bidding samples (364 tobacco flavors) were discriminated quickly and accurately. The models could characterize the similarity between the bidding samples and the standard samples, which was consistent with the results of chromatographic fingerprint analysis. The method is fast, accurate, practical, and suitable for quick evaluation of the quality of flavors and fragrances in bidding.

     

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